Microstructures
by George Langford, Sc.D., Massachusetts Institute of Technology, Cambridge, MA, 1966
Copyright©
2005 by George Langford
Surface Coatings and Heat Resisting Alloys - Lesson 3 - Second specimen
Cement mixer shaft at 200X etched
The user of this cement mixer shaft demanded that the steelmaker replace the shaft after it failed.

The first photomicrograph shows the transition zone between a surface layer and the base metal (AISI 4140 steel) at 200X magnification.

The shaft appears to have been "built up" (enlarged) by flame spraying with a low carbon steel, which is to the right in this image.  The surface of the shaft has a cast, ferritic microstructure; underneath is a carbon diffusion zone; and then there is a layer of (brown) martensite.

There were MnS stringers visible in the microstructure, indicating the wrought nature of the original shaft.
Flame sprayed mixer shaft at 500X etched
The second photomicrograph, shown at 500X at left, resolves the cast microstructure of the built-up layer along with a large crack, which was probably the result of transformation stresses during cooling (martensitic transformation of the outer portion of the hardenable 4140 substrate metal) after the spraying process.

How do I know that I haven't got this image upside down with respect to the first image ?



The answer to this question is below.



























Answer:  There is a cold shut to the right of center.  The apparent colors of the microstructure often change with different magnifications.
Specimen 3 is nichrome, a heat resisting alloy.