This photomicrograph was taken at 200X, and the next one is
at 1000X. The etchant was ammonium peroxide - hydrogen
peroxide. The material is copper. How was this microwave guide formed ? Why would you say it was not cast ? The wave guide was made on a pattern made from poly(methyl methacrylate) - PMMA - and coated with silver. It was then electroplated heavily with copper from a copper sulphate bath. This particular specimen was removed from the bath several times, producing a layered structure. |
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The bent "annealing" twins are indicative of a highly
faulted and strained microstructure, a result of the high deposition
rate necessary to form such a massive electrodeposited thickness (six
millimeters). Note the absence of any normal grain structure, the
columnar grains, and the lack of porosity. This excellent microstructure was produced by a process called electroforming (no endorsement intended). The silver was leached away by acid treatment from the inside of the waveguide after removing the PMMA with a solvent. Specimen 9 is next on the agenda. |